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Avaliação sistemática do efeito de matriz em ensaios bioanalíticos por LC-MS/MS para a análise de rifampicina em fluidos biológicos
(Universidade Federal de São Carlos, 2011-04-29)
Bioanalytical assays by LC-MS/MS were conducted in order to investigate the
matrix effect (ME) in the analysis of rifampicin (RIF) in biological matrices, human
plasma or microsomal fractions, which were submitted to ...
Determinação sequencial rápida de As e Sb, Bi e Pb por espectrometria de absorção atômica com geração de hidretos
(Universidade Federal de São Carlos, 2012-03-22)
In this study it was developed two systems, one for the fast sequencial determination of As and Sb and other for Bi and Pb using flame atomic absorption spectrometry with hydride generation. To optimize the system for the ...
Desenvolvimento de método analítico com emprego da espectrometria de absorção atômica para a determinação de Cd, Fe, Pb e Zn em amostras de interesse alimentício
(Universidade Federal de São Carlos, 2008-07-31)
Analytical chemistry plays a fundamental role in proposing fast and reliable procedures to analyze food samples. Proper selection and introduction of complementary foods reduces the vulnerability to micronutrient deficiencies. ...
Avaliação do comportamento de BTEX e seus metabólitos de biodegradação em solos: estudos de remedição em microcosmos
(Universidade Federal de São Carlos, 2015-08-28)
The monoaromatic hydrocarbons composed by benzene, toluene, ethylbenzene and xylenes isomers (BTEX), are commonly found near local oil refineries, filling stations, or around pipelines, as a result ofleaks and/or spills. ...
Avaliação das condições operacionais de espectrômetro de emissão óptica com plasma acoplado indutivamente com configuração axial
(Universidade Federal de São Carlos, 2007-02-23)
The goal of this thesis was the critical
evaluation of the analytical capability of an inductively coupled plasma spectrometer
(ICP OES) with axially viewed configuration. The general view that axially systems are mainly ...
Eletrodo de diamante dopado com boro para a determinação voltamétrica/amperométrica de antihelmínticos e anti-hipertensivos
(Universidade Federal de São Carlos, 2014-06-27)
In this work it was developed, firstly, one method for determination of anthelmintic albendazole (ABZ) using differential pulse voltammetry (DPV) and the boron doped diamond (BDD) electrode catholically pretreated (BDD-CPT). ...
Análise foliar de plantas por espectrometria de emissão óptica com plasma induzido por laser (LIBS) e com plasma acoplado indutivamente após ablação com laser (LA-ICP OES)
(Universidade Federal de São Carlos, 2013-09-20)
It has been demonstrated that laser induced breakdown spectrometry (LIBS) can be used as an alternative method for the determination of macro (P, K, Ca, Mg) and micronutrients (B, Fe, Cu, Mn, Zn) in pellets of plant ...
Produção e caracterização de material de referência de forrageira para nutrientes e contaminantes inorgânicos
(Universidade Federal de São Carlos, 2013-04-12)
The main aim of this work was to produce a candidate material for national reference material, the forage Brachiaria brizantha Stapf. cv. Marandu, containing known levels of contaminants (Cr, Pb, Cd, and As) and macro and ...
Tratamento metrológico e quimiométrico de dados de ressonância magnética nuclear para amostras de biodiesel em diesel
(Universidade Federal de São Carlos, 2012-03-29)
The development of instrumentation in Nuclear Magnetic Resonance (NMR) increased the sensitivity of the technique, allowing samples in micro and nanogram scale can be examined. These new technologies enabled the NMR technique ...
Especiação química de As e Cd por HPLC-ICP-MS em forrageira Brachiaria brizantha Stapf. cv. Marandu cultivada em solo previamente contaminado
(Universidade Federal de São Carlos, 2014-03-21)
Recent research and advances in analytical chemistry show that the total content determination of an element, although it is essential, is limited since it is not sufficient to provide information about the bioavailability ...