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Now showing items 31-40 of 56
Construção e aplicação analítica de espectrômetro de emissão atômica com atomização eletrotérmica em filamento de tungstênio
(Universidade Federal de São Carlos, 2011-02-04)
This thesis has two lines of development based on measurements of atomic emission using a tungsten coil electrothermal atomizer. The first line dealt with the construction of a tungsten coil atomic emission spectrometer ...
Avaliação sistemática do efeito de matriz em ensaios bioanalíticos por LC-MS/MS para a análise de rifampicina em fluidos biológicos
(Universidade Federal de São Carlos, 2011-04-29)
Bioanalytical assays by LC-MS/MS were conducted in order to investigate the
matrix effect (ME) in the analysis of rifampicin (RIF) in biological matrices, human
plasma or microsomal fractions, which were submitted to ...
Determinação sequencial rápida de As e Sb, Bi e Pb por espectrometria de absorção atômica com geração de hidretos
(Universidade Federal de São Carlos, 2012-03-22)
In this study it was developed two systems, one for the fast sequencial determination of As and Sb and other for Bi and Pb using flame atomic absorption spectrometry with hydride generation. To optimize the system for the ...
Desenvolvimento de procedimento para determinação fotométrica de etanol em bebidas destiladas sem uso de reagentes explorando o efeito Schlieren
(Universidade Federal de São Carlos, 2015-07-23)
The knowledge and applications of Schlieren effect on the flow injection analysis process (FIA) showed that using the variation of refraction index, formed by concentration gradients during sample dispersion in carrier ...
Especiação redox de crômio em amostras de solos contaminados
(Universidade Federal de São Carlos, 2012-03-21)
Chromium and its compounds are employed in various industrial processes, and these activities are responsible for the disposal of significant amounts of materials containing this element in the environment. Due to the known ...
Quantificação de resíduos de amoxicilina e ampicilina por injeção direta de amostras de leite de bovino
(Universidade Federal de São Carlos, 2011-12-07)
The development of new methods for analysis and quantification of drugs and their metabolites in biological fluids is of great interest in various areas of knowledge. The pre-treatment of complex matrices is a fundamental ...
Avaliação da qualidade de um córrego urbano com relação às espécies metálicas e hidrocarbonetos policíclicos aromáticos (HPA)
(Universidade Federal de São Carlos, 2012-02-16)
Frequent use of urban waters for public supply has been increased, due to reduction of water resources suitable for human consumption. These waters are exposed to point and non-point sources of pollution, such as, atmospheric ...
Aplicação de espectroscopia raman e análise multivariada na caracterização e monitoramento in situ da síntese de cocristais de carbamazepina-nicotinamida e ibuprofenonicotinamida
(Universidade Federal de São Carlos, 2014-02-20)
In this work, the PAT tools were used (Raman spectroscopy with an in situ analyzer and multivariate tools) to proceed a crystallization monitoring and quantification of cocrystals of carbamazepine nicotinamide (CBZ NCT) ...
Metabolismo in vitro do albendazol em escala miligrama e purificação por cromatografia líquida de alta eficiência semipreparativa
(Universidade Federal de São Carlos, 2012-06-06)
This work presents the in vitro metabolism of albendazole (ABZ) conducted with microsomal fractions obtained from Wistar rats and performed in analytical and semipreparative scale. Subsequent separation and purification ...
Preparo e caracterização de material de referência de solo para nutrientes e contaminantes inorgânicos
(Universidade Federal de São Carlos, 2014-09-26)
The certified reference materials make an important role in the establishment of traceability in analytical chemistry, ensuring reliability and accuracy to the measurements and are fundamental for the validation of analytical ...