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Desenvolvimento de métodos analíticos empregando a espectrometria de absorção atômica sequencial rápida com atomização em chama
(Universidade Federal de São Carlos, 2012-06-01)
The aim of this PhD thesis was to develop analytical methods employing fast sequential flame atomic absorption spectrometry (FS-FAAS). In the first part of this study, a fast and simple method is proposed for the determination ...
Espectrometria de Emissão Atômica em Filamento de Tungstênio (WCAES) : potencialidades e aplicações
(Universidade Federal de São Carlos, 2012-11-14)
This thesis describes the analytical application of WCAES for the determination of Ca, Al, Cs, Sr and Cr in samples with different compositions. In all studies the observation zone of the detector related to the coil was ...
Especiação redox de crômio em amostras de solos contaminados
(Universidade Federal de São Carlos, 2012-03-21)
Chromium and its compounds are employed in various industrial processes, and these activities are responsible for the disposal of significant amounts of materials containing this element in the environment. Due to the known ...
Complexos fosfínicos de Ru(II) e Ru(III) com fármacos anti-tuberculose e seus derivados
(Universidade Federal de São Carlos, 2012-05-25)
In this work were synthesized ruthenium complexes using pyrazinamide (PZA), a first-line drug in the treatment of tuberculosis, as well as isonicotinamide (ins) and isonicotinic acid (INA), isoniazid derivatives, as ligand. ...
Influência da adição de nitrato de cálcio e de PhoslockTM no abatimento dos fluxos de nutrientes e metais na interface sedimento-coluna de água em um sistema lacustre eutrofizado
(Universidade Federal de São Carlos, 2012-02-16)
This research project evaluated the changes in the fluxes of nutrients
and metals at the sediment-water interface as a result of sediment treatment by the
additions of PhoslockTM and calcium nitrate solution. The experiments ...
Identificação e estudo do fungo Mucor circinelloides isolado do tronco de Pinus taeda, com ênfase em biotransformação da carvona
(Universidade Federal de São Carlos, 2012-03-28)
Identification and study of the fungus Mucor circinelloides isolated from the trunk of Pinus taeda, with emphasis on the carvone biotransformation. Fungi associated with plants have been studied ripping seeking the discovery ...
Estudo da variação de pH interfacial durante a reação de desprendimento de hidrogênio por simulação de elementos finitos
(Universidade Federal de São Carlos, 2012-02-27)
Different papers propose a interfacial pH variation during an electrochemical reaction. Among them, as example, can be cited the electrodeposition of Zn and Co as well as the steel corrosion in aqueous sulphide solutions. ...
Determinação de molibdênio em plantas combinando microextração e espectrometria de absorção atômica em chama
(Universidade Federal de São Carlos, 2012-08-16)
In this study, a procedure for the determination of low concentrations of molybdenum in plants by flame atomic absorption spectrometry (FAAS) was developed. The poor sensitivity of FAAS for determination of refractory ...
Estudo de reações sólido/líquido e sólido/gás em altas temperaturas: o caso das reações do PbSO4EPbO no processo pirometalúrgico de reciclagem de Pb a partir de baterias chumbo-ácido
(Universidade Federal de São Carlos, 2012-02-10)
This report presents a study on there reactions and transformations occurring at high temperatures with the two main constituents of scrap lead-acid batteries (Pb/H2SO4) oxide and lead sulphate (PbSO4 and PbO). It was ...
Mapa de caracterização do texto científico : produção e funcionamento em disciplinas de química do ensino superior
(Universidade Federal de São Carlos, 2012-01-24)
The main objectives of this research were to develop and to implement a tool ‐ the Characterization Map of Scientific Text ‐ which could assist students in recognizing the structural and rhetorical aspects of ...