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Desenvolvimento de modelos de calibração multivariada em espectroscopia de infravermelho próximo para ácidos graxos em amostras de carne bovina
(Universidade Federal de São Carlos, 2016-03-21)
The Brazilian cattle have shown promise prominence in the international market
compared to other commodities. It already knows the important role of fatty acids in the complimentarily of human nutrition. On the other hand, ...
Determinação de molibdênio em plantas combinando microextração e espectrometria de absorção atômica em chama
(Universidade Federal de São Carlos, 2012-08-16)
In this study, a procedure for the determination of low concentrations of molybdenum in plants by flame atomic absorption spectrometry (FAAS) was developed. The poor sensitivity of FAAS for determination of refractory ...
Determinação de metais por técnicas espectroanalíticas em amostras de carne e sangue de bovinos submetidos à dieta com adição de erva-mate (Ilex paraguariensis, St. Hilaire)
(Universidade Federal de São Carlos, 2016-05-23)
Given the importance of quality in the bovine meat and its relationship with the diet submitted to animals, this master dissertation has the proposition to evaluate the Ca, Cu, Fe, K, Mg, and Zn concentrations changes in ...
Determinação de arsênio total e inorgânico em sucos de frutas e arroz por ICP-MS
(Universidade Federal de São Carlos, 2016-07-07)
Analytical procedures using inductively coupled plasma mass spectrometry (ICP-MS) for the determination of total As in rice samples and fruit juices and inorganic As in rice samples were developed. A microwave-assisted ...
Estudo do perfil químico de Cyperus rotundus e avaliação do seu potencial de absorção de metais
(Universidade Federal de São Carlos, 2016-07-27)
The following work describes the comparative study of the variation between chemical profiles of plants of the Cyperus rotundus species – where one was collected at Vale S.A.’s dumping ground in Canaã dos Carajás city, ...
Novas arquiteturas para sensores modificados com materiais nanoestruturados de carbono
(Universidade Federal de São Carlos, 2016-02-19)
In this work are reported the development of new architectures for sensors using carbon nanomaterials. Firstly, the investigation of the nanomaterials reduced graphene oxide (RGO) and carbon black (CB) in
chitosan film ...
Tris(trimethylsilyl)silane and visible-light irradiation : a new metal- and additive-free photochemical process for the synthesis of indoles and oxindoles
(Universidade Federal de São Carlos, 2016-07-29)
A combined tris(trimethylsilyl)silane and visible-light-promoted intramolecular reductive cyclization protocol for the synthesis of indoles and oxindoles has been developed (Scheme 1).1 This straightforward and efficient ...
Desenvolver a cidadania através da química : é possível? Um desafio a ser vencido
(Universidade Federal de São Carlos, 2003-12-17)
The present work was inspired by the High School National
Curriculum Parameters (PCNEM) as well the Schnetzler proposal of teaching
chemistry to citizenship. It is also based on the observed chemistry teaching
problems, ...
Quantificação de metacrilatos residuais e avaliação da liberação em saliva artificial a partir de resinas acrílicas para reembasamento imediato
(Universidade Federal de São Carlos, 2008-05-21)
This work reports the development of analytical methods, using High Performance of Liquid Chromatography (HPLC), to quantify unreacted monomers from dental reline autopolimerizing acrylic resins. The quantification of these ...
Desenvolvimento de estratégias para a determinação espectrofotométrica sequencial em fluxo de Co (II) e Mn (II)
(Universidade Federal de São Carlos, 2009-07-24)
In this study a kinetic-spectrophotometric method was developed for sequential determination of Co and Mn in pharmaceutical samples. The method was based on the catalytic effect of the analytes in the oxidation reaction ...