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Síntese, caracterização e testes eletroquímicos de dióxido de manganês nanométrico como material de eletrodo de supercapacitores
(Universidade Federal de São Carlos, 2018-08-01)
Manganese dioxide was synthesized by a microwave-hydrothermal method using alternative, unprecedented and completely soluble reagents. For such, potassium permanganate and acetone were dissolved in different proportions ...
Desenvolvimento de uma nova rota de síntese hidrotermal assistida por micro-ondas para a obtenção de nanopartículas de espinélios de manganês e lítio dopados com alumínio para aplicação em baterias de íons lítio
(Universidade Federal de São Carlos, 2018-03-01)
Spinel of manganese and lithium undoped and doped with aluminum were obtained by an unpublished, energy saving, short time, and low temperature synthesis: microwave-assisted hydrothermal route. Undoped spinel was synthesized ...
Estudo mecanístico de reações de estado sólido: o caso do sistema Pb/PbSO4/Na2SO4
(Universidade Federal de São Carlos, 2012-11-21)
In this work, the growth and reduction of PbSO4 in Na2SO4 solution under transient conditions was characterized. A novel methodology for the working-electrode surface preparation before stabilization enhanced the voltametric ...
Síntese eletroquímica e caracterização de filmes finos de Sb2Se3
(Universidade Federal de São Carlos, 2017-12-05)
Due to the environmental appeal, the shortage of raw material and the chemical complexity of some systems employed at photovoltaic devices, interest has been growing for semiconductors composed of abundant, low toxicity ...
Síntese de LiFePO4 em sistema hidrotermal assistido por micro-ondas, caracterização e testes como catodo de baterias de íons lítio
(Universidade Federal de São Carlos, 2018-07-30)
Different routes for lithium iron phosphate (LiFePO4) synthesis were studied in a microwave-assisted hydrothermal system in order to reduce the time and temperature of synthesis in relation to the traditional methods of ...
Instabilidades em eletrocatálise: cinética complexa catalisada por superfícies modelo
(Universidade Federal de São Carlos, 2018-02-28)
The electro-oxidation of small molecules is an area of great interest due to its application in energy converting systems, such as fuel cells. The reactions present in these systems involve several reaction pathways - which ...
Contra eletrodos de sulfetos metálicos aplicados a células solares sensibilizadas por pontos quânticos
(Universidade Federal de São Carlos, 2019-05-22)
The quantum dot-sensitized solar cells (CSSPQ) are considered as third generation solar cell, derived from dye-sensitized solar cells (CSSC). Several works in the literature shown that the optimization of counter electrodes ...
Efeitos térmicos durante a foto-eletro-oxidação de glicerol catalisada por CdS
(Universidade Federal de São Carlos, 2019-10-25)
Cadmium sulfide (CdS) is one of the most important chalcogenides applied to water splitting, which has a band gap of 2.4 eV that suits very well with the solar spectrum. Moreover, CdS possesses a strong reduction activity ...