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Laser-induced breakdown spectroscopy (LIBS), wavelength dispersive x-ray fluorescence (WDXRF) and chemometrics: possibilities for analytical applications in food analysis
(Universidade Federal de São Carlos, 2020-07-14)
This PhD thesis proposes evaluation of the possibilities and analytical applications of the laser-induced breakdown spectroscopy (LIBS) and wavelength dispersive x-ray fluorescence (WDXRF) techniques for the determination ...
Calibração multivias em Laser-Induced Breakdown Spectroscopy (LIBS) para determinação de Ca, K e Mg em amostras de suplemento mineral para humanos
(Universidade Federal de São Carlos, 2021-03-25)
This work intends to present a new approach for modeling LIBS data resolved in time using multiway algorithms, aiming to achieve the advantage of second order. The algorithms evaluated in this study were: Multivariate Curve ...
Eletrodo de pasta de carbono modificado com solvente eutético profundo hidrofóbico e sua aplicação voltamétrica
(Universidade Federal de São Carlos, 2021-03-01)
In this work, the use of hydrophobic deep eutectic solvent was proposed for the modification of carbon paste electrodes. Different HDES were prepared using fatty acids: octanoic, decanoic, and dodecanoic acids, and ...
Biorrefinaria aplicada à cadeia de soja: um estudo de caso de extração verde e sustentável de isoflavonas
(Universidade Federal de São Carlos, 2021-04-29)
SOY BIOREFINERY: GREEN AND SUSTAINABLE EXTRACTION OF ISOFLAVONES. Brazil has the potential to be the world's largest producer of soybeans (Glycine max), being, in 2020, responsible for the production of 124 Mt of oilseeds. ...
Quantificação e caracterização de microplásticos na atmosfera de São Carlos – SP
(Universidade Federal de São Carlos, 2022-11-25)
With the rampant use of plastics, combined with the annual increase in its production, a large generation of waste is often incorrectly disposed of, resulting in plastic pollution in the environment, including macro, micro, ...
Reaproveitamento de resíduos agroindustriais de frutas obtidos por meio de manejo convencional e orgânico: estudo de métodos para a extração verde e sustentável de compostos bioativos
(Universidade Federal de São Carlos, 2022-03-31)
The magnitude of the Brazilian agricultural and agro industrial market impresses by its greatness, but it is also the cause of serious concerns regarding the amount of waste generated and how to handle such residues. This ...
Deconvolução de espectros UV diretamente de soluções de degradação forçada de fármacos
(Universidade Federal de São Carlos, 2022-04-27)
Forced degradation studies (EDFs) are assays which pharmaceuticals are placed under stress conditions, which include acidic, basic, oxidative, high temperature, photodegradation, humidity and metal ions environments. The ...
Supramolecular synthesis and characterization of new multicomponent forms of fluconazole
(Universidade Federal de São Carlos, 2020-06-30)
Active Pharmaceutical Ingredient (API) is the therapeutic constituent that defines the pharmacological properties and performance of the drug. Their qualities vary due to their respective physicochemical and pharmacological ...
Utilização de técnicas espectro analíticas para avaliação de açúcar de cana-de-açúcar
(Universidade Federal de São Carlos, 2021-06-16)
Brazil is the largest sugarcane producer in the world, and its consolidated industry also
places it in the position of the largest producer and exporter of sugar. With a highly
variable process and also with large ...
Desenvolvimento de métodos de pré-concentração para a determinação de elementos traço e especiação de cromo e arsênio em amostras agrícolas
(Universidade Federal de São Carlos, 2021-10-27)
Agricultural sustainable production is indispensable to meet the growing demand for food and nutritional control. The risk assessment associated with contamination by toxic elements in agricultural and aquaculture matrices ...