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Avaliação sistemática do efeito de matriz em ensaios bioanalíticos por LC-MS/MS para a análise de rifampicina em fluidos biológicos
(Universidade Federal de São Carlos, 2011-04-29)
Bioanalytical assays by LC-MS/MS were conducted in order to investigate the
matrix effect (ME) in the analysis of rifampicin (RIF) in biological matrices, human
plasma or microsomal fractions, which were submitted to ...
Determinação sequencial rápida de As e Sb, Bi e Pb por espectrometria de absorção atômica com geração de hidretos
(Universidade Federal de São Carlos, 2012-03-22)
In this study it was developed two systems, one for the fast sequencial determination of As and Sb and other for Bi and Pb using flame atomic absorption spectrometry with hydride generation. To optimize the system for the ...
Avaliação do comportamento de BTEX e seus metabólitos de biodegradação em solos: estudos de remedição em microcosmos
(Universidade Federal de São Carlos, 2015-08-28)
The monoaromatic hydrocarbons composed by benzene, toluene, ethylbenzene and xylenes isomers (BTEX), are commonly found near local oil refineries, filling stations, or around pipelines, as a result ofleaks and/or spills. ...
Eletrodo de diamante dopado com boro para a determinação voltamétrica/amperométrica de antihelmínticos e anti-hipertensivos
(Universidade Federal de São Carlos, 2014-06-27)
In this work it was developed, firstly, one method for determination of anthelmintic albendazole (ABZ) using differential pulse voltammetry (DPV) and the boron doped diamond (BDD) electrode catholically pretreated (BDD-CPT). ...
Análise foliar de plantas por espectrometria de emissão óptica com plasma induzido por laser (LIBS) e com plasma acoplado indutivamente após ablação com laser (LA-ICP OES)
(Universidade Federal de São Carlos, 2013-09-20)
It has been demonstrated that laser induced breakdown spectrometry (LIBS) can be used as an alternative method for the determination of macro (P, K, Ca, Mg) and micronutrients (B, Fe, Cu, Mn, Zn) in pellets of plant ...
Produção e caracterização de material de referência de forrageira para nutrientes e contaminantes inorgânicos
(Universidade Federal de São Carlos, 2013-04-12)
The main aim of this work was to produce a candidate material for national reference material, the forage Brachiaria brizantha Stapf. cv. Marandu, containing known levels of contaminants (Cr, Pb, Cd, and As) and macro and ...
Tratamento metrológico e quimiométrico de dados de ressonância magnética nuclear para amostras de biodiesel em diesel
(Universidade Federal de São Carlos, 2012-03-29)
The development of instrumentation in Nuclear Magnetic Resonance (NMR) increased the sensitivity of the technique, allowing samples in micro and nanogram scale can be examined. These new technologies enabled the NMR technique ...
Especiação química de As e Cd por HPLC-ICP-MS em forrageira Brachiaria brizantha Stapf. cv. Marandu cultivada em solo previamente contaminado
(Universidade Federal de São Carlos, 2014-03-21)
Recent research and advances in analytical chemistry show that the total content determination of an element, although it is essential, is limited since it is not sufficient to provide information about the bioavailability ...
Emprego de imagens hiperspectrais e espectrometria de emissão em plasma introduzido por laser na análise direta de amostras de lixo eletrônico
(Universidade Federal de São Carlos, 2015-02-27)
In this study, laser induced breakdown spectroscopy was combined with chemometric
tools to study the chemical composition of WEEE discarded. For this, three
samples of printed circuit board were chosen for analysis: PCBs ...
Estratégias espectroanalíticas para análise química inorgânica de plantas medicinais
(Universidade Federal de São Carlos, 2014-12-01)
This thesis describes the development of analytical procedures based on direct solid analysis by high-resolution continuum source atomic absorption spectrometry in graphite furnace (SS-HR-CS GF AAS) and aqueous solutions ...