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Determinação sequencial rápida de As e Sb, Bi e Pb por espectrometria de absorção atômica com geração de hidretos
(Universidade Federal de São Carlos, 2012-03-22)
In this study it was developed two systems, one for the fast sequencial determination of As and Sb and other for Bi and Pb using flame atomic absorption spectrometry with hydride generation. To optimize the system for the ...
Estudo mecanístico de reações de estado sólido: o caso do sistema Pb/PbSO4/Na2SO4
(Universidade Federal de São Carlos, 2012-11-21)
In this work, the growth and reduction of PbSO4 in Na2SO4 solution under transient conditions was characterized. A novel methodology for the working-electrode surface preparation before stabilization enhanced the voltametric ...
Busca por novos metalofármacos contra doenças negligenciadas (malária, doença de chagas e leishmaniose)
(Universidade Federal de São Carlos, 2012-07-13)
Leishmaniasis, Chagas disease and malaria are neglected parasitic diseases responsible for high mortality in tropical low-income countries. Due to the lack of vaccines and of safe, effective and affordable treatments, there ...
Síntese de clorinas anfifílicas com potenciais aplicações em terapia fotodinâmica
(Universidade Federal de São Carlos, 2012-10-26)
The main objective of this work was to construct amphiphilic chlorins with low aggregation in a physiological environment. The synthesis and structural characterization of the target compounds were carried out, and preliminary ...
A regioquímica das reações de Diels-Alder de N-tosil para-benzoquinona iminas
(Universidade Federal de São Carlos, 2012-02-29)
In this work it was done a comparative study on the reactivity of a variety of dienophiles including para-benzoquinones, their mono-oximes, their N-tosyl mono-oximes and their N-tosylimines on the Diels-Alder reactions ...
Influência dos íons Cu2+ nas propriedades ópticas dos pós de (Ca1-x Cux)TiO3 preparados por métodos químicos
(Universidade Federal de São Carlos, 2012-10-29)
The influence of Cu2+ doping as well as the preparation methods on the structural, morphological and optical properties of (Ca1-xCux)TiO3 powders with (x= 0; 0,01; 0,02; 0,04 and 0,10) of Cu2+ were studied in this work. ...
Tratamento metrológico e quimiométrico de dados de ressonância magnética nuclear para amostras de biodiesel em diesel
(Universidade Federal de São Carlos, 2012-03-29)
The development of instrumentation in Nuclear Magnetic Resonance (NMR) increased the sensitivity of the technique, allowing samples in micro and nanogram scale can be examined. These new technologies enabled the NMR technique ...
Estudo do crescimento e automontagem de nanocristais coloidais
(Universidade Federal de São Carlos, 2012-12-07)
In the last two decades a remarkable progress in nanomaterials knowledge has been done, mainly in the chemical synthesis of inorganic nanocrystals via colloidal processes. Several of these advances addressed the growth ...
Síntese e investigações estruturais de arranjos supramoleculares formados por metaloporfirinas e metaloftalocianinas
(Universidade Federal de São Carlos, 2012-06-29)
This thesis involves the syntheses and characterization of four heterotriads formed by metallotetraphenylporphyrins (CoTPP and NiTPP) and metallophthalocyanines (CoPc and NiPc) using pyrazine (pz) and trans-1,2-bis(4-pyr ...
Uso de imagens digitais e ferramentas quimiométricas para identificação e determinação de Cr (VI) em solos contaminados
(Universidade Federal de São Carlos, 2012-03-23)
The determination of toxic metals in soils is an important factor to access their quality or identify possible contamination. The element Cr has double feature: Cr (III) is essential for human beings and Cr (VI) is toxic. ...