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Nanomateriais semicondutores aplicados na fabricação de dispositivos eletroquímicos
(Universidade Federal de São Carlos, 2019-03-22)
This dissertation was subdivided into 3 different studies. In the first study, it was proposed the development of a photo-electrochemical system for the removal of caffeine in natural water samples. Photo-anodes made with ...
Fotocatálise e suas aplicações em reações de ciclização oxidativa e terapia fotônicas
(Universidade Federal de São Carlos, 2019-05-06)
In the chapter 1, studies on photocatalysed reactions were carried out by porphyrins and other photocatalysts aiming at the formation of radicals in amino aromatic systems for subsequent addition reaction. More specifically, ...
Cinética de fotodegradação natural de contaminantes emergentes em ETE aeróbia
(Universidade Federal de São Carlos, 2019-02-26)
The advances in sample preparation and analytical detection techniques made possible the evaluation of a new class of contaminants found in the ug L-1 – ng L-1 range, known as Emerging Contaminants (EC). Along with that, ...
Complexos de cobre (II) de bases de Schiff prolínicas aplicados como inibidores e miméticos funcionais da enzima Urease e à formação de 1,2,3-triazóis 1,4-dissubstituídos
(Universidade Federal de São Carlos, 2019-03-18)
In this work five Schiff base-type ligands derived from a series of reaction steps were
synthesized starting from the amino acid L-proline, in which four of them are novel
and were completely characterized by 1H, 13C, ...
Arginase: da imobilização à modulação de ensaios de afinidade em coleções de produtos naturais
(Universidade Federal de São Carlos, 2019-05-17)
ARGINASE: FROM THE IMMOBILIZATION TO MODULATION OF AFFINITY ASSAY IN COLLECTIONS OF NATURAL PRODUCTS. The use of natural products from plants dates from antiquity and they are often targets as they exhibit biological ...
Síntese de acil fosfodiésteres por mecanoquímica: uma metodologia de química verde
(Universidade Federal de São Carlos, 2019-08-22)
Green chemistry is very concerned with the sustainability of chemical reactions, where one of the objectives, which in the formulation/remodeling of synthetic routes can replace toxic solvents with solvents of lower toxicity, ...
Efeitos térmicos durante a foto-eletro-oxidação de glicerol catalisada por CdS
(Universidade Federal de São Carlos, 2019-10-25)
Cadmium sulfide (CdS) is one of the most important chalcogenides applied to water splitting, which has a band gap of 2.4 eV that suits very well with the solar spectrum. Moreover, CdS possesses a strong reduction activity ...
Desenvolvimento de filmes biodegradáveis baseados em pectina e nanofibras de celulose funcionalizadas
(Universidade Federal de São Carlos, 2019-08-26)
Renewable polymers are an interesting alternative to synthetic polymers from petrochemical sources. The work aims at the development of nanocomposite films based on pectin and functionalized cellulose nanofibers. The ...
Estudo microestrutural dos contornos de grão em estágio inicial de formação no sistema cerâmico ZnO-Bi2O3
(Universidade Federal de São Carlos, 2019-08-28)
Polycrystalline materials have solid-solid interfaces known as grain boundary. These interfaces have long been treated as just a region of defects between the crystals (grains), but recent studies have shown that such ...
Síntese, caracterização e estudos de citotoxicidade e alvo biológico de complexos quadráticos planos contendo Tiossemicarbazonas
(Universidade Federal de São Carlos, 2019-09-20)
The diversity of cancer diseases and the side effects caused by the drugs commonly used in cancer treatment require different antineoplasic agents able to operate more specific and in a way to minimize the side effects. ...