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Aplicação de imagens digitais e técnicas espectroanalíticas combinadas com quimiometria para detecção e quantificação de adulteração em leite bovino
(Universidade Federal de São Carlos, 2013-02-22)
Milk provides essential nutrients (carbohydrate, fat, protein, minerals and vitamins) of great nutritional relevance for humans, particularly during childhood. Nowadays, the occurrence of milk adulteration is a major issue ...
Estratégias analíticas para a avaliação química de solos e liquens da Antártica marítima
(Universidade Federal de São Carlos, 2011-08-12)
The aim of this PhD thesis is the ample study of soil and lichen samples from Antarctica, collected in regions under strong anthropogenic impact. Surface soil samples were collected around several scientific stations: ...
Estratégias quimiométricas para análise de plantas por espectrometria de emissão óptica com plasma induzido por laser
(Universidade Federal de São Carlos, 2010-12-08)
A simultaneous optimization strategy based on neuro-genetic approach is proposed for selection of operational parameters for the simultaneous determination of macronutrients (Ca, Mg and P), micronutrients (B, Cu, Fe, Mn ...
Teores dos elementos químicos essenciais e tóxicos na rastreabilidade da carne bovina
(Universidade Federal de São Carlos, 2012-02-15)
The objective of this work was to develop methodologies for the determination of inorganic constituents in meat sample and the study of correlations between samples with chemical elements profile, especially Nelore samples ...
Avaliação da espectrometria de emissão óptica com plasma induzido por laser (LIBS) para a determinação de Ba, Cd, Cr e Pb em brinquedos
(Universidade Federal de São Carlos, 2010-11-17)
LIBS is a spectroanalytical technique that employs the microsampling by laser ablation and subsequent exitations for atoms, ions and molecular fragments presents in induced microplasm.This technique was evaluated for ...
Aplicação de espectroscopia raman e análise multivariada na caracterização e monitoramento in situ da síntese de cocristais de carbamazepina-nicotinamida e ibuprofenonicotinamida
(Universidade Federal de São Carlos, 2014-02-20)
In this work, the PAT tools were used (Raman spectroscopy with an in situ analyzer and multivariate tools) to proceed a crystallization monitoring and quantification of cocrystals of carbamazepine nicotinamide (CBZ NCT) ...
Estudo da viabilidade do uso de métodos de segunda ordem e RMN na elaboração de fingerprint de bauhinia forficata baseado em seu extrato bruto
(Universidade Federal de São Carlos, 2014-10-30)
Given the large number of species of Bauhinia and great morphological similarity between them, it is necessary the development of robust analytical techniques in quality control of plants used as herbal medicines, since ...
Emprego de imagens hiperspectrais e espectrometria de emissão em plasma introduzido por laser na análise direta de amostras de lixo eletrônico
(Universidade Federal de São Carlos, 2015-02-27)
In this study, laser induced breakdown spectroscopy was combined with chemometric
tools to study the chemical composition of WEEE discarded. For this, three
samples of printed circuit board were chosen for analysis: PCBs ...
Uso de imagens digitais e ferramentas quimiométricas para identificação e determinação de Cr (VI) em solos contaminados
(Universidade Federal de São Carlos, 2012-03-23)
The determination of toxic metals in soils is an important factor to access their quality or identify possible contamination. The element Cr has double feature: Cr (III) is essential for human beings and Cr (VI) is toxic. ...
Tratamento metrológico e quimiométrico de dados de ressonância magnética nuclear para amostras de biodiesel em diesel
(Universidade Federal de São Carlos, 2012-03-29)
The development of instrumentation in Nuclear Magnetic Resonance (NMR) increased the sensitivity of the technique, allowing samples in micro and nanogram scale can be examined. These new technologies enabled the NMR technique ...