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Cerâmicas de PZT modificadas com terras raras sintetizadas usando o método dos complexos oxidantes de peróxido (OPM) e sinterizadas por micro-ondas
(Universidade Federal de São Carlos, 2013-07-23)
The Pb(Zr0,52Ti0,48)O3 solid solution in morphotropic phase and its modified (RExPb1-x)(Zr0,52Ti0,48O3) with RE = La, Pr or Nd and x = 0.05, 0.10, 0.15, 0.20, 0.30, 0.38 and 0.45 were satisfctorily prepared by oxidant ...
Síntese, caracterização e deposição sobre óxido de grafeno de nanopartículas de óxido de índio dopado com estanho (ITO)
(Universidade Federal de São Carlos, 2011-11-22)
In this study, in the first step, Indium tin oxide nanoparticles were synthesized via a non-aqueous route involving the solvothermal treatment of indium (III) acetylacetonate and tin (IV) chloride in polyethylene glycol ...
Nanopartículas coloidais de ouro e prata e sua funcionalização com dibutil-dicalcogenetos
(Universidade Federal de São Carlos, 2010-02-25)
Hybrid materials present interesting combination of the physical and chemical properties of organic and inorganic compounds in a single material that is widely employed in distinct technological applications. In the present ...
Nanocristais de TiO2 : relação entre parâmetros morfológicos, estruturais e fotocatálise
(Universidade Federal de São Carlos, 2010-02-26)
In this work, morphologically different TiO2 nanocrystals were synthesized through the OPM method with the objective of performing a comparative study related to photoactivity. Morphological characterization was performed ...
Desenvolvimento de nanocompósitos baseados em hidrogéis aplicados à liberação de nutrientes agrícolas
(Universidade Federal de São Carlos, 2014-03-21)
Nanocomposites were developed based on polyacrylamide hydrogels (PAAm) and methylcellulose (MC) reinforced with montmorillonite (MMT), undergoing the materials to subsequent hydrolysis process and evaluating their loading ...
Método solvotérmico assistido por micro-ondas aplicado à obtenção de nanocristais de ITO : deposição e caracterização de filmes de ITO
(Universidade Federal de São Carlos, 2012-02-17)
The formation of In1-xSnxO2 (ITO) nanocrystals through the conversion of radiant energy into heat has been studied by using an adapted domestic microwave oven. The formation of powder was obtained by heating the oven to ...
Estudo das propriedades fotoluminescentes do ZnS e ZnS: Eu obtidos pelo método solvotérmico assistido por microondas
(Universidade Federal de São Carlos, 2012-07-20)
This paper is about the synthesis, characterization and studies of nanostructures of ZnS and ZnS:Eu3+ prepared by microwave-assisted solvothermal method. The influence of the synthesis time in the microwave on the samples ...
Determinação simultânea de íons metálicos por meio de técnicas eletroanalíticas e quimiométricas
(Universidade Federal de São Carlos, 2011-05-19)
In this work, the determination of three metallic ions was performed, namely Zn2+, Cd2+ and Pb2+, in very different concentration range, from _g/L until mg/L, using differential pulse anodic stripping voltammetry over ...
Estudo do efeito isotópico sobre a solubilidade da 3- metilpiridina em H2O e D2O
(Universidade Federal de São Carlos, 2012-12-07)
Experimental studies of 3-methylpiridyne/water and 3- methylpiridyne/heavy water binary mixtures show solubility differences. In this work Molecular Dynamics method was used to simulate 54 model systems. Each system ...
Estudo da atividade eletrocatalítica de multicamadas metálicas de Ir/Pt e Cu/Pt eletrodepositadas sobre Pt(policristalina) para eletrooxidação de moléculas orgânicas pequenas
(Universidade Federal de São Carlos, 2013-09-26)
The search for alternative energy sources stead fossil fuel has driven the development of new energy generating devices. Among these, the Direct Alcohol Fuel Cells are a kind of device that directly convert chemical energy ...