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Catálise por complexos metálicos: I – Complexos de Ni(II), Cu(II) e Pd(II) com bases de Schiff na oxidação de catecóis; II – Complexos de Ru(II) com ligantes tipo-pinça na desidrogenação de álcoois
(Universidade Federal de São Carlos, 2021-06-11)
Green Chemistry is an indispensable scientific tool for sustainable development, catalysis is one of its twelve principles through which energy waste and hazardous chemicals production can be minimized. In this sense, ...
Determinação de impurezas inorgânicas em medicamentos: avaliação de preparo de amostra e medidas espectroanalíticas
(Universidade Federal de São Carlos, 2021-06-16)
Green sample preparation procedures were developed in this dissertation for determination of elemental impurities in drugs and dietary supplements by argon-based plasma spectroanalytical methods according to Chapters 232, ...
Busca de substâncias inseticidas e fungicidas para controle de formigas-cortadeiras através do estudo fitoquímico biomonitorado de espécies de Picramnia e avaliação da atividade bacteriostático em Xanthomonas citri subsp citri
(Universidade Federal de São Carlos, 2019-10-31)
The search for insecticide and fungicide substances to control leaf-cutting ants through biomonitored phytochemical study of Picramnia species and evaluation of bacteriostatic activity in Xanthomonas citri. Subsp citri. ...
Planejamento experimental aplicado aos estudos de degradação forçada do fármaco Ticagrelor
(Universidade Federal de São Carlos, 2020-08-31)
Stability indicating tests are an essential part during pharmaceutical drug production, besides being a mandatory step for the regulation and approval from the regulatory agencies. Forced degradation consist of an exposure ...
Obtenção de sulfetos metálicos (M= Ni, Mo) pelo método solvotermal assistido por micro-ondas aplicados na reação de desprendimento de hidrogênio
(Universidade Federal de São Carlos, 2020-03-27)
In general, transition metal sulfides show good activity in the Hydrogen Evolution Reaction (HER). Some of these metals, such as Mo and Ni, arouse interest in the area of electrocatalysis, since they are more abundant and ...
Estudo espectroscópico por FTIR da conversão de etanol em catalisadores de Au suportados
(Universidade Federal de São Carlos, 2020-07-25)
In this work, an FTIR spectroscopic study of gold catalysts supported on monoclinic zirconia (with Au content of 2,5% w/w), was carried out in order to elucidate the surface nature of this catalyst in the dehydrogenation ...
Síntese de miméticos da urease de Canavalia ensiformis e avaliação mecanística da decomposição da ureia
(Universidade Federal de São Carlos, 2020-02-20)
Urease is a metalloenzyme found in many different organisms, which is also associated to virulence factors, such as pielonefritis. Hence, the study of urease inhibitors is necessary to control its activity. For a better ...
Mecanismos reacionais dos sistemas Pb/H2SO4 e Pb/PbO2/H2SO4
(Universidade Federal de São Carlos, 2012-01-26)
The thesis will address a modern view of electrochemistry for the discharge and charge reactions of Lead Acid Batteries study. Even though these batteries have existed for more than 200 years, electrochemical mechanisms ...
Desenvolvimento de dispositivo microfluídico descartável contendo arranjos de biossensores para a determinação multiplexada de espécies de interesse biológico em diferentes matrizes
(Universidade Federal de São Carlos, 2020-10-30)
16 sensing points for the construction of an array of biosensors. The components of this device have been individually evaluated and their construction design has been optimized for the best performance of the sensors. ...
Flow chemistry applied to hazardous reactions, and fluorophores synthesis with photophysics studies
(Universidade Federal de São Carlos, 2020-02-20)
Two distinct cases of continuous flow conditions applied to dangerous reactions are described. The first example is the continuous photooxygenation of a series of dienes that produces endoperoxides and / which are potentially ...