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Determinação de polifenóis totais utilizando sistemas de análise por injeção em fluxo.
(Universidade Federal de São Carlos, 2004-02-17)
In this dissertation, three flow injection analysis methods for total polyphenol
determination in tea and acacia s tannins commercial extracts were developed. The first method is based on the reaction between the polyphenol ...
Espectroscopia Raman amplificada por superfície associada à cromatografia em camada delgada para análise de amostras alimentícias
(Universidade Federal de São Carlos, 2018-04-13)
Surface enhancement Raman spectroscopy (SERS) presents the advantages of conventional Raman spectroscopy with the possibility to detect compounds in low levels due to the enhancement on Raman intensity, generated by the ...
Avaliação de polímeros impressos para pré- concentração/extração de Se, U e Cd
(Universidade Federal de São Carlos, 2015-06-18)
This thesis describes the development of imprinted polymers for preconcentration of Se, Cd and U. The relevant factors to the FIA system and preconcentration were optimized by Doehlert matrix. Chapter I describes an ...
Desafios na análise de benzofenonas em leite materno por injeção direta de amostras usando cromatografia líquida hifenada à espectrometria de massa
(Universidade Federal de São Carlos, 2018-08-30)
As a solution to the paradigm of achieving maximum efficiency in a shorter analysis time, Ultra High-performance Liquid Chromatography (UHPLC) coupled to mass spectrometry (MS / MS) have been successfully explored. The ...
Avalição química e da capacidade de biossorção da grama batatais (Paspalum notatum) visando aplicações analíticas.
(Universidade Federal de São Carlos, 2004-09-03)
This work suggests the chemical characterization of the genus Paspalum and was divided in 3 steps: 1) sample preparation of plants with diluted acids; 2) biosorption studies employing
Paspalum notatum root material, and ...
Estudo do mecanismo de oxidação do herbicida atrazina na presença de minerais e sustâncias húmicas em ambiente anaeróbio.
(Universidade Federal de São Carlos, 2005-12-14)
The oxidative decomposition of atrazine was induced by hydroxyl radicals generated from the interaction between hydrogen peroxide, H2O2, and iron oxides, yielding the
Fenton reaction. The reaction rate of atrazine oxidation ...
Influência de íons metálicos na estrutura de substâncias húmicas detectados por espectroscopia.
(Universidade Federal de São Carlos, 2005-03-23)
INFLUENCE OF METAL CATIONS IN THE STRUCTURE OF
HUMIC SUBSTANCES AS DETECTED BY SPECTROSCOPY, involves a
study by which starting from precursors of humic substances, some polymers
were obtained, characterized and comparable ...
Desenvolvimento de métodos para determinação de metilbrometo de homatropina em produtos farmacêuticos empregando turbidimetria em fluxo e titulação condutimétrica.
(Universidade Federal de São Carlos, 2004-07-23)
Antimuscarinic compounds are drugs, which play important role on the central nervous system. The most widely used are atropine, escopolamine, homatropine and homatropine methylbromide. These drugs are utilized in several ...
Diferenciação química de quatro espécies de Bauhinia (pata-de-vaca)
(Universidade Federal de São Carlos, 2018-06-15)
The search for new compounds from natural products with high biological activity is an arduous task that has improved due to the evolution of instrumental analytical techniques. In addition, the use of medicinal herbs for ...
Estudo da influência do glicerol no processo de deposição de ligas Zn-Mn e nos depósitos de Zn-Mn
(Universidade Federal de São Carlos, 2011-02-18)
The influence of glycerol additive on the electrodeposition process of Zn-Mn on Pt substrate from acid baths by means of cyclic voltammetry and the characteristics of the coatings by Scanning Electron Microscopy (SEM), ...